Doncaster suffer first league defeat at Belper
The hosts led 2-0 at half time before James Gunthorpe halved the deficit.
Andy Appleton failed to level from a penalty stroke and Belper made the Town Field side pay by going 4-1 up.
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Hide AdTravis Creswell and Tim Shelley netted to make it 4-3 but the hosts killed the game off by scoring when Doncaster had two players sin-binned.
Doncaster, who dropped to third in the table, host Timperley on Sunday (2pm).
Doncaster’s ladies lost 3-0 at home to Conference North leaders Sutton Coldfield and are yet to get off the mark this season.
They travel to Beeston on Saturday.